Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Glycidol → 3-(Octadecylamino)propane-1,2-diol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Glycidol | HCID 11164 | — |
| 반응물 | Octadecylamine | HCID 15793 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3-(Octadecylamino)propane-1,2-diol | HCID 120088 | — |
반응 단계
Octadecylamine (9.09 g, 0.034 mole) was dissolved in absolute ethanol. Glycidol (5.00 g, 0.068 mole) was added to the amine dropwise. The reaction solution was refluxed under nitrogen for 4 hours and then was stirred overnight at room temperature. A white solid was obtained (crude yield=10.8 g). The solid was recrystalized from hot hexane. (Yield=6.9 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05476671 |
| 출처 데이터셋 | uspto-grants-1995_12 |
| ORD ID | ord-2093b14d28454a6cadc580b9c2ddb3ce |
| 출처 메모 | uspto-grants-1995_12 |