Trimethylamine → Indoline, 1-(2-(4-pyridyl)ethyl)-

HRID 2261497노트

반응식

HRID 2261497 반응식
[OH-].[Na+].[CH3:3][CH2:4][CH:5]([CH:7](NC([C@H]1O[C@@H]1C(O)=O)=O)[C:8]([NH:10][CH2:11][CH2:12][CH2:13][CH2:14]N)=O)[CH3:6].C[N:26]([CH3:28])C>O>[CH2:13]1[C:12]2[C:11](=[CH:3][CH:4]=[CH:5][CH:6]=2)[N:10]([CH2:8][CH2:7][C:5]2[CH:4]=[CH:3][N:26]=[CH:28][CH:6]=2)[CH2:14]1

참가 물질

5

반응물 3

HCID 1146TrimethylamineHCID 14798Sodium HydroxideHCID 101946933HCID 101946933, 화합물

생성물 1

HCID 25056Indoline, 1-(2-(4-pyridyl)ethyl)-

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Another core-shell polymer, according to the present invention, was prepared by combining 200 g of SP-1 with 533 g of demineralized water and adjusting the pH to 10 with sodium hydroxide. The mixture was combined with 267 g of CPI-2 and stirred for 30 minutes. 59.1 g of trimethylamine (25% aq.) were added and allowed to stir for one hour. After one hour, the pH was raised to 12 and the mixture was vacuum distilled for 3 hours to remove residual trimethylamine.

후처리

  1. customwas prepared
  2. stirringto stir for one hour
  3. waitAfter one hour
  4. temperaturethe pH was raised to 12
  5. distillationdistilled for 3 hours
  6. customto remove residual trimethylamine

출처 및 근거

ORD 기록
ord-ed2d412eb0504b7390f004de5cbfe877
출처 데이터셋
uspto-grants-2010_12
특허 번호
US07847027B2

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