Glyoxylic Acid → HCID 68679422, 화합물

HRID 2265900노트

반응식

[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([NH:11][CH2:12][CH2:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=2[O:20][CH2:21][CH2:22][N:23]2[CH2:28][CH2:27][CH2:26][CH2:25][CH2:24]2)(=[O:10])=[O:9])=[CH:4][CH:3]=1.[C:29]([OH:33])(=[O:32])[CH:30]=O>>[N:23]1([CH2:22][CH2:21][O:20][C:15]2[CH:16]=[CH:17][CH:18]=[C:19]3[C:14]=2[CH2:13][CH2:12][N:11]([S:8]([C:5]2[CH:4]=[CH:3][C:2]([CH3:1])=[CH:7][CH:6]=2)(=[O:10])=[O:9])[CH:30]3[C:29]([OH:33])=[O:32])[CH2:28][CH2:27][CH2:26][CH2:25][CH2:24]1

참가 물질

반응물 2

HCID 760Glyoxylic Acid

HCID 68681197HCID 68681197, 화합물

생성물 1

HCID 68679422HCID 68679422, 화합물

실험 절차

4-Methyl-N-{2-[2-(2-piperidin-1-ylethoxy)phenyl]ethyl}benzenesulfonamide is reacted with glyoxylic acid in analogy to the method described for Example 20.

출처 및 근거

ORD 기록: ord-fb8f94ff75ec45168dfc77697ca1a14f
출처 데이터셋: uspto-grants-2010_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07858619B2

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