Hydrochloric Acid → 1,4-Diazepan-2-one hydrochloride

HRID 227247

반응식

HRID 227247 반응식
[O:1]=[C:2]1[NH:8][CH2:7][CH2:6][CH2:5][N:4](C(OC(C)(C)C)=O)[CH2:3]1.[ClH:16]>O1CCOCC1>[ClH:16].[NH:8]1[CH2:7][CH2:6][CH2:5][NH:4][CH2:3][C:2]1=[O:1]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 21962087tert-Butyl 3-oxo-1,4-diazepane-1-carboxylate

생성물 1

HCID 234475441,4-Diazepan-2-one hydrochloride

시약·촉매·용매 1

HCID 312751,4-Dioxane용매

실험 절차

Compound from Step B was treated with 4 N hydrogen chloride in dioxane at ambient temperature for 2.5 h. Concentration gave the title compound.

후처리

  1. concentrationConcentration

출처 및 근거

ORD 기록
ord-9334e80c14c045b58a60d9f0a1165788
출처 데이터셋
uspto-grants-2009_07
특허 번호
US07560455B2

연결된 노트

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