Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → p-Trifluoromethoxybenzaldehyde oxime
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | p-(Trifluoromethoxy)benzaldehyde | HCID 69573 | — |
| 반응물 | Hydroxyamine hydrochloride | HCID 443297 | — |
| 생성물 | p-Trifluoromethoxybenzaldehyde oxime | HCID 2777199 | 94% |
반응 단계
In a similar manner as described in Preparation Example 1, by using 4-(trifluoromethoxy)benzaldehyde (38.02 g, 200.0 mmol), sodium hydroxide (12.00 g, 300.0 mmol) and hydrochloric acid hydroxylamine (16.68 g, 240 mmol), a white solid required compound (38.68 g, 188 mmol, 94%) was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09132126B2 |
| 출처 데이터셋 | uspto-grants-2015_09 |
| ORD ID | ord-2d1b21b657f145ceb454501707d3938c |
| 출처 메모 | uspto-grants-2015_09 |