Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyl Sulfoxide → Anisole, m-pentadecyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyl Sulfoxide | HCID 679 | — |
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Hydrogenated cardanol | HCID 68146 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Anisole, m-pentadecyl- | HCID 578947 | — |
반응 단계
To a two necked round bottomed flask with a reflux condenser is added 3-pentadecyl phenol, DMSO, sodium hydroxide followed by dropwise addition of alkylating agent such as methyl iodide with constant stirring at room temperature. The stirring is continued for about 6-8 hrs. The reaction mixture is then poured into deionized water and the organic matter is extracted in diethyl ether, separated the organic layer, washed with water and dried, purified to obtain 3-pentadecyl anisole.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09133089B2 |
| 출처 데이터셋 | uspto-grants-2015_09 |
| ORD ID | ord-0cadd41262b44dd289521f0f2f868abf |
| 출처 메모 | uspto-grants-2015_09 |