Cyclopentanone → Ethyl 3-(cyclopentylamino)-2,2-dimethylpropanoate

반응식

[CH2:1]([O:3][C:4](=[O:10])[C:5]([CH3:9])([CH3:8])[CH2:6][NH2:7])[CH3:2].[C:11]1(=O)[CH2:15][CH2:14][CH2:13][CH2:12]1.C([O-])(=O)C.[Na+].C(O[BH-](OC(=O)C)OC(=O)C)(=O)C.[Na+]>C(Cl)Cl>[CH2:1]([O:3][C:4](=[O:10])[C:5]([CH3:9])([CH3:8])[CH2:6][NH:7][CH:11]1[CH2:15][CH2:14][CH2:13][CH2:12]1)[CH3:2]

참가 물질

실험 절차

Reaction of 3-amino-2,2-dimethyl-propionic acid ethyl ester with cyclopentanone, sodium acetate and sodium triacetoxyborohydride in DCM gave 3-Cyclopentylamino-2,2-dimethyl-propionic acid ethyl ester

출처 및 근거

ORD 기록: ord-2b2b721d5b8a488b9e99df8e784d6cb1
출처 데이터셋: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09133199B2

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참가 물질

반응물 4

HCID 8452Cyclopentanone

HCID 421529Ethyl 3-amino-2,2-dimethylpropanoate

HCID 517045Sodium Acetate

HCID 5049666Sodium triacetoxyborohydride

생성물 1

HCID 57969950Ethyl 3-(cyclopentylamino)-2,2-dimethylpropanoate

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

Reaction of 3-amino-2,2-dimethyl-propionic acid ethyl ester with cyclopentanone, sodium acetate and sodium triacetoxyborohydride in DCM gave 3-Cyclopentylamino-2,2-dimethyl-propionic acid ethyl ester

출처 및 근거

ORD 기록: ord-2b2b721d5b8a488b9e99df8e784d6cb1
출처 데이터셋: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09133199B2

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불러오는 중…