Oxalyl chloride → 2,3-Dichloro-6-iodobenzoic acid chloride
반응식
[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[C:7]([I:12])[C:3]=1[C:4](O)=[O:5].C(Cl)(=O)C([Cl:16])=O>CN(C=O)C.C(OCC)(=O)C>[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[C:7]([I:12])[C:3]=1[C:4]([Cl:16])=[O:5]참가 물질
5
실험 절차
DMF (one drop) was added to a stirred solution of 2,3-dichloro-6-iodobenzoic acid (1.53 g, 4.83 mmol) and oxalyl chloride (2 ml) in ethyl acetate (20 ml). After 2 hours, the solution was evaporated and the product was used immediately.
후처리
- customthe solution was evaporated
출처 및 근거
- ORD 기록
- ord-fcb6181488fb4a4085cac970464cc3d3
- 출처 데이터셋
- uspto-grants-2000_07
- 특허 번호
- US06083952
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