Oxalyl chloride → 2,3-Dichloro-6-iodobenzoic acid chloride

HRID 2287343

반응식

HRID 2287343 반응식
[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[C:7]([I:12])[C:3]=1[C:4](O)=[O:5].C(Cl)(=O)C([Cl:16])=O>CN(C=O)C.C(OCC)(=O)C>[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[C:7]([I:12])[C:3]=1[C:4]([Cl:16])=[O:5]

참가 물질

5

반응물 2

HCID 65578Oxalyl chlorideHCID 220088162,3-Dichloro-6-iodobenzoic acid

생성물 1

HCID 542920312,3-Dichloro-6-iodobenzoic acid chloride

시약·촉매·용매 2

HCID 6228Dimethylformamide촉매HCID 8857Ethyl Acetate용매

실험 절차

DMF (one drop) was added to a stirred solution of 2,3-dichloro-6-iodobenzoic acid (1.53 g, 4.83 mmol) and oxalyl chloride (2 ml) in ethyl acetate (20 ml). After 2 hours, the solution was evaporated and the product was used immediately.

후처리

  1. customthe solution was evaporated

출처 및 근거

ORD 기록
ord-fcb6181488fb4a4085cac970464cc3d3
출처 데이터셋
uspto-grants-2000_07
특허 번호
US06083952

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