Hydrochloric Acid → 1,3,5-Tris-(p-(oct-1-yloxycarbonyl)-anilino)-s-triazine

HRID 2290601

반응식

HRID 2290601 반응식
[NH2:1][C:2]1[CH:18]=[CH:17][C:5]([C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])=[O:7])=[CH:4][CH:3]=1.[N:19]1[C:26](Cl)=[N:25][C:23](Cl)=[N:22][C:20]=1Cl.Cl>C1(C)C(C)=CC=CC=1>[CH2:9]([O:8][C:6]([C:5]1[CH:4]=[CH:3][C:2]([NH:1][N:19]2[CH2:26][N:25]([NH:1][C:2]3[CH:18]=[CH:17][C:5]([C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])=[O:7])=[CH:4][CH:3]=3)[CH2:23][N:22]([NH:1][C:2]3[CH:3]=[CH:4][C:5]([C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])=[O:7])=[CH:17][CH:18]=3)[CH2:20]2)=[CH:18][CH:17]=1)=[O:7])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 7954Cyanuric chlorideHCID 26629Octyl p-aminobenzoate

생성물 1

HCID 201527331,3,5-Tris-(p-(oct-1-yloxycarbonyl)-anilino)-s-triazine

시약·촉매·용매 1

HCID 7237O-Xylene용매

반응 조건

온도
90 °C

실험 절차

75 g of octyl p-aminobenzoate and 18.5 g of cyanuric chloride in 1,000 ml of xylene were heated at 140° C. for 8 hours. After the evolution of hydrogen chloride was complete, the reaction solution was cooled to 90° C., washed twice with saturated sodium bicarbonate solution and once with water and then cooled to room temperature. The white crystals precipitated were filtered off under suction.

후처리

  1. washwashed twice with saturated sodium bicarbonate solution and once with water
  2. temperaturecooled to room temperature
  3. customThe white crystals precipitated
  4. filtrationwere filtered off under suction

출처 및 근거

ORD 기록
ord-406a8ee66c394100acc9d9181a37e888
출처 데이터셋
uspto-grants-1986_10
특허 번호
US04617390

연결된 노트

불러오는 중…