Hydrochloric Acid → HCID 20031799, 화합물
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C([O:4][C:5]1[CH:24]=[CH:23][C:8]([C:9]([O:11][C:12]2[C:17]([F:18])=[C:16]([F:19])[C:15]([F:20])=[C:14]([F:21])[C:13]=2[F:22])=[O:10])=[CH:7][CH:6]=1)(=O)C.Cl>O1CCCC1>[OH:4][C:5]1[CH:24]=[CH:23][C:8]([C:9]([O:11][C:12]2[C:13]([F:22])=[C:14]([F:21])[C:15]([F:20])=[C:16]([F:19])[C:17]=2[F:18])=[O:10])=[CH:7][CH:6]=1참가 물질
4
실험 절차
Pentafluorophenyl 4-acetoxybenzoate (10 g) in tetrahydrofuran was treated with 50 ml of 5M hydrochloric acid and 150 ml of tetrahydrofuran and stirred at room temperature overnight. The solvents were evaporated in vacuo to give a product which was purified by column chromatography (silica; ethyl acetate/hexane mixtures as eluant) to afford the title compound (8 g).
후처리
- customThe solvents were evaporated in vacuo
- customto give a product which
- customwas purified by column chromatography (silica; ethyl acetate/hexane mixtures as eluant)
출처 및 근거
- ORD 기록
- ord-f0eba863e7a149a8a74543afb0be07cc
- 출처 데이터셋
- uspto-grants-1989_01
- 특허 번호
- US04795748
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