Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Succinamide → 1-(2-Bromoethyl)pyrrolidine-2,5-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Succinamide | HCID 8036 | — |
| 반응물 | 1,1-Dibromoethane | HCID 11201 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 용매 | Methyl Ethyl Ketone | HCID 6569 | — |
| 생성물 | 1-(2-Bromoethyl)pyrrolidine-2,5-dione | HCID 13561395 | — |
반응 단계
49.5 g of succinamide was dissolved in 750 ml of 2-butanone under heating. 187.9 g of dibromoethane and 138 g of anhydrous potassium carbonate were added to the solution and the mixture was heated under reflux for 9.5 h.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04801603 |
| 출처 데이터셋 | uspto-grants-1989_01 |
| ORD ID | ord-c828f9b75a7a408abe6987fc6ce65114 |
| 출처 메모 | uspto-grants-1989_01 |