Methacryloyl chloride → 4-Benzoylphenyl methacrylate
반응식
[OH:1][C:2]1[CH:15]=[CH:14][C:5]([C:6]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:7])=[CH:4][CH:3]=1.[C:16](Cl)(=[O:20])[C:17]([CH3:19])=[CH2:18]>N1C=CC=CC=1>[C:16]([O:1][C:2]1[CH:3]=[CH:4][C:5]([C:6]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:7])=[CH:14][CH:15]=1)(=[O:20])[C:17]([CH3:19])=[CH2:18]참가 물질
4
실험 절차
Prepared from 6.0 g of 4-hydroxybenzophenone and 4.4 ml of methacryloyl chloride in 70 ml of pyridine. Recrystallized from ethyl acetate-ethanol-water; M.P.~69.5°-70.5° C.
후처리
- customRecrystallized from ethyl acetate-ethanol-water
출처 및 근거
- ORD 기록
- ord-1acdee1fb46248e9a9aa8eaed28885da
- 출처 데이터셋
- uspto-grants-1989_01
- 특허 번호
- US04801610
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