3,3-Dimethyl-1-butanol → HCID 57438253, 화합물

HRID 229473

반응식

HRID 229473 반응식
[CH3:1][C:2]([CH3:7])([CH3:6])[CH2:3][CH2:4][OH:5].[ClH:8].[NH2:9][CH2:10][C:11](=[O:17])[CH2:12][CH2:13][C:14](O)=[O:15]>>[ClH:8].[NH2:9][CH2:10][C:11](=[O:17])[CH2:12][CH2:13][C:14]([O:5][CH2:4][CH2:3][C:2]([CH3:7])([CH3:6])[CH3:1])=[O:15]

참가 물질

3

반응물 2

HCID 122333,3-Dimethyl-1-butanolHCID 123608Aminolevulinic Acid Hydrochloride

생성물 1

HCID 57438253HCID 57438253, 화합물

실험 절차

From 3,3-dimethyl-1-butanol (5.0 g; 49 mmol) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol) at 70° C. The reaction was complete after 4 h. The yield was 0.91 g (60%), mp146-148°.

후처리

  1. customat 70° C

출처 및 근거

ORD 기록
ord-81830e3d96334285927ebb672f08ddcc
출처 데이터셋
uspto-grants-2009_07
특허 번호
US07563819B1

연결된 노트

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