Bromine → HCID 22597763, 화합물

HRID 2297622노트

반응식

HRID 2297622 반응식
[CH3:1][O:2][C:3]1[CH:11]=[C:10]([CH:12]([CH3:14])[CH3:13])[CH:9]=[CH:8][C:4]=1[C:5]([OH:7])=[O:6].[Br:15]Br>C(Cl)(Cl)Cl>[Br:15][C:9]1[C:10]([CH:12]([CH3:14])[CH3:13])=[CH:11][C:3]([O:2][CH3:1])=[C:4]([CH:8]=1)[C:5]([OH:7])=[O:6]

참가 물질

4

반응물 2

HCID 24408BromineHCID 126137372-Methoxy-4-(propan-2-yl)benzoic acid

생성물 1

HCID 22597763HCID 22597763, 화합물

시약·촉매·용매 1

HCID 6212Chloroform용매2회

실험 절차

To a solution of 2-methoxy-4-iso-propyl benzoic acid (7.0 g 36.0 mmol) in chloroform (100 ml) was added bromine (1.86 ml) in chloroform (20 ml) dropwise. The reaction was stirred at room temperature overnight. Evaporation in vacuo afforded an oil (9.27 g).

후처리

  1. customEvaporation in vacuo

출처 및 근거

ORD 기록
ord-567255e82caa4e7e8c1ffbb3330aaf69
출처 데이터셋
uspto-grants-2002_12
특허 번호
US06492378B1

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