Phenyl Isothiocyanate → 3-(2-furyl)-4-phenyl-5-{[4-(trifluoromethyl)benzyl]thio}-4H-1,2,4-triazole

HRID 229767

반응식

HRID 229767 반응식
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]([NH:8][NH2:9])=O.[C:10]1([N:16]=[C:17]=[S:18])[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.[F:19][C:20]([F:30])([F:29])[C:21]1[CH:28]=[CH:27][C:24]([CH2:25]Br)=[CH:23][CH:22]=1>>[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1[N:16]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[C:17]([S:18][CH2:25][C:24]2[CH:23]=[CH:22][C:21]([C:20]([F:19])([F:29])[F:30])=[CH:28][CH:27]=2)=[N:9][N:8]=1

참가 물질

4

반응물 3

HCID 7673Phenyl IsothiocyanateHCID 187312-Furancarboxylic acid, hydrazideHCID 1230621-(Bromomethyl)-4-(trifluoromethyl)benzene

생성물 1

HCID 462249923-(2-furyl)-4-phenyl-5-{[4-(trifluoromethyl)benzyl]thio}-4H-1,2,4-triazole

실험 절차

This compound was synthesized using the same methodology as described in Example 1 above, using 2-furancarboxylic acid hydrazide, phenyl isothiocyanate and 4-trifluoromethylbenzyl bromide as the starting materials. (M+H)+−402.

후처리

  1. customThis compound was synthesized

출처 및 근거

ORD 기록
ord-f144a6c0943640a5a762f1ba94b83ff7
출처 데이터셋
uspto-grants-2009_07
특허 번호
US07563905B2

연결된 노트

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