Trimethylolpropane diallyl ether → 2,2-Bis[(allyloxy)methyl]butanal

HRID 2299056

반응식

HRID 2299056 반응식
[CH2:1]([O:4][CH2:5][C:6]([CH2:11][O:12][CH2:13][CH:14]=[CH2:15])([CH2:9][CH3:10])[CH2:7][OH:8])[CH:2]=[CH2:3].C(Cl)(=O)C(Cl)=O>CS(C)=O>[CH2:13]([O:12][CH2:11][C:6]([CH2:5][O:4][CH2:1][CH:2]=[CH2:3])([CH2:9][CH3:10])[CH:7]=[O:8])[CH:14]=[CH2:15]

참가 물질

4

반응물 2

HCID 61196Trimethylolpropane diallyl etherHCID 65578Oxalyl chloride

생성물 1

HCID 183797072,2-Bis[(allyloxy)methyl]butanal

시약·촉매·용매 1

HCID 679Dimethyl Sulfoxide용매

실험 절차

2,2-Bis(allyloxymethyl)-1-butanol, oxalyl chloride and dimethylsulfoxide were processed as described in Example 18A to provide the title compound.

출처 및 근거

ORD 기록
ord-23fa92039a064785aca70685ef42f6eb
출처 데이터셋
uspto-grants-2002_12
특허 번호
US06495576B2

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