Ethanol → 2-(4-Methoxyphenyl)-1,1-dimethylethylamine
반응식
C[C:2]1[CH:7]=[CH:6][C:5]([CH2:8][C:9]([CH3:14])([N+:11]([O-])=O)[CH3:10])=[CH:4][CH:3]=1.[H][H].[CH2:17]([OH:19])C>[Ni]>[CH3:10][C:9]([NH2:11])([CH3:14])[CH2:8][C:5]1[CH:6]=[CH:7][C:2]([O:19][CH3:17])=[CH:3][CH:4]=1참가 물질
5
실험 절차
The 1-(4-methylphenyl)-2-methyl-2-nitropropane (1.3 g) was hydrogenated for 5 hours at 65 p.s.i. hydrogen in ethanol (30 mL) using 1.4 g of Raney nickel as catalyst. Removal of the catalyst by filtration and evaporation of the solvent yielded 1.15 g of 1,1-dimethyl-2-(4-methoxyphenyl)ethylamine as a clear oil.
후처리
- customRemoval of the catalyst
- filtrationby filtration and evaporation of the solvent
출처 및 근거
- ORD 기록
- ord-b6ce9e958be945119df15bd49ef620b2
- 출처 데이터셋
- uspto-grants-2002_08
- 특허 번호
- US06432656B1
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