반응식
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:14][CH2:13][CH2:12][N:11](C(OC(C)(C)C)=O)[CH2:10][CH2:9]2)=[CH:4][C:3]=1[NH:22][S:23]([C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1)(=[O:25])=[O:24].[CH2:32]([S:34]([Cl:37])(=[O:36])=[O:35])[CH3:33]>>[ClH:37].[N:8]1([C:5]2[CH:6]=[CH:7][C:2]([NH:1][S:34]([CH2:32][CH3:33])(=[O:36])=[O:35])=[C:3]([NH:22][S:23]([C:26]3[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=3)(=[O:24])=[O:25])[CH:4]=2)[CH2:14][CH2:13][CH2:12][NH:11][CH2:10][CH2:9]1참가 물질
3
실험 절차
N-{5-(1,4-diazepan-1-yl)-2-[(ethylsulfonyl)amino]phenyl}benzenesulfonamide hydrochloride was synthesized from N-{2-amino-5-(4-t-butyloxycarbonyl-1,4-diazepan-1-yl)-phenyl}benzenesulfonamide (0.085 g, 0.19 mmol) and ethanesulfonyl chloride (0.032 μL, 0.25 mmol) to give 29.1 mg of a light purple solid; Anal. (C24H27ClN4O3S×0.75H2O) C, H, N, S.; M+ 439.4 Calcd 439.14.
출처 및 근거
- ORD 기록
- ord-a7cb56248f08475fa37dbcab33467709
- 출처 데이터셋
- uspto-grants-2009_07
- 특허 번호
- US07566715B2
연결된 노트
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