Sodium → HCID 86593394, 화합물

HRID 2308055노트

반응식

HRID 2308055 반응식
[CH3:1][C:2]1[C:7]([CH3:8])=[CH:6][CH:5]=[CH:4][C:3]=1[C:9]#[CH:10].[Cl:11][C:12]1[CH:19]=[C:18]([O:20][CH3:21])[CH:17]=[CH:16][C:13]=1[CH2:14][SH:15].[Na]>>[CH3:1][C:2]1[C:7]([CH3:8])=[CH:6][CH:5]=[CH:4][C:3]=1/[CH:9]=[CH:10]\[CH:14]([S:15][CH:14](/[CH:10]=[CH:9]\[C:3]1[CH:4]=[CH:5][CH:6]=[C:7]([CH3:8])[C:2]=1[CH3:1])[C:13]1[CH:16]=[CH:17][C:18]([O:20][CH3:21])=[CH:19][C:12]=1[Cl:11])[C:13]1[CH:16]=[CH:17][C:18]([O:20][CH3:21])=[CH:19][C:12]=1[Cl:11]

참가 물질

4

반응물 3

HCID 5360545SodiumHCID 226037641-Ethynyl-2,3-dimethylbenzeneHCID 22603791HCID 22603791, 화합물

생성물 1

HCID 86593394HCID 86593394, 화합물

실험 절차

A solution of 2,3-dimethylphenylacetylene (0.02 mol), 2-chloro-4-methoxybenzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) is subjected to the General Procedure to form (Z)-2,3-dimethylstyryl-2-chloro-4-methoxybenzylsulfide. The title compound is obtained following oxidation of the sulfide, according to the General Procedure.

출처 및 근거

ORD 기록
ord-c9b5a36046f64035a89549bf9a7bf527
출처 데이터셋
uspto-grants-2004_12
특허 번호
US06833480B2

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