Methacrylic Acid → Methyl 2-methylprop-2-enoate;2-methylprop-2-enoic acid

HRID 2309148

반응식

HRID 2309148 반응식
[C:1]([O:6][CH3:7])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:8]([OH:13])(=[O:12])[C:9]([CH3:11])=[CH2:10].CC(C(C(C(S)(C)C)(C)C)(C)C)C.C(OOC(=O)CCCCCCCCCCC)(=O)CCCCCCCCCCC>>[C:1]([O:6][CH3:7])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:8]([OH:13])(=[O:12])[C:9]([CH3:11])=[CH2:10]

참가 물질

5

반응물 4

HCID 4093Methacrylic AcidHCID 6658Methyl MethacrylateHCID 7773Lauroyl peroxideHCID 32793Tert-dodecanethiol

생성물 1

HCID 65310Methyl 2-methylprop-2-enoate;2-methylprop-2-enoic acid

실험 절차

A solution comprising 90 parts by weight of methyl methacrylate, 10 parts by weight of methacrylic acid, 0.75 part by weight of tert-dodecylmercaptan, and 0.4 part by weight of lauroyl peroxide was prepared. A methyl methacrylate/methacrylic acid copolymer was formed from this solution in the same manner as described in Example 8.

후처리

  1. customwas prepared

출처 및 근거

ORD 기록
ord-5fb856e4e9b54f0dab4c0d6899221736
출처 데이터셋
uspto-grants-1987_09
특허 번호
US04693553

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