Methyl iodide → 2-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyltrimethylammonium iodide

HRID 231264노트

반응식

HRID 231264 반응식
[CH3:1][O:2][CH:3]([CH2:13][O:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH2:4][S:5]([CH2:8][CH2:9][N:10]([CH3:12])[CH3:11])(=[O:7])=[O:6].[CH3:33][I:34]>CCOCC>[I-:34].[CH3:1][O:2][CH:3]([CH2:13][O:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH2:4][S:5]([CH2:8][CH2:9][N+:10]([CH3:33])([CH3:12])[CH3:11])(=[O:6])=[O:7]

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 144982652-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyldimethylamine

생성물 1

HCID 144982482-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyltrimethylammonium iodide

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

In 5 ml of ether is dissolved 0.24 g of 2-[(2-methoxy-3-octadecyloxypropyl)sulfonyl]ethyldimethylamine to which is added 1 ml of methyl iodide. The solution is then stirred at room temperature for 2 days. The reaction liquid is concentrated under reduced pressure and the residue is treated with methanol to give 275 mg of the captioned compound as powder.

후처리

  1. customThe reaction liquid
  2. concentrationis concentrated under reduced pressure
  3. additionthe residue is treated with methanol

출처 및 근거

ORD 기록
ord-c41443b41d0f4024954fde2ad444d8d1
출처 데이터셋
uspto-grants-1989_07
특허 번호
US04845219

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