Phenol, 4-[2-(4-nitrophenyl)ethenyl]- → 6-{4-[2-(4-Nitrophenyl)ethenyl]phenoxy}hexan-1-OL

HRID 232188

반응식

HRID 232188 반응식
[K].[OH:2][C:3]1[CH:8]=[CH:7][C:6]([CH:9]=[CH:10][C:11]2[CH:16]=[CH:15][C:14]([N+:17]([O-:19])=[O:18])=[CH:13][CH:12]=2)=[CH:5][CH:4]=1.I[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][OH:27]>>[OH:27][CH2:26][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH:9]=[CH:10][C:11]2[CH:16]=[CH:15][C:14]([N+:17]([O-:19])=[O:18])=[CH:13][CH:12]=2)=[CH:5][CH:4]=1

참가 물질

4

반응물 3

HCID 139676Phenol, 4-[2-(4-nitrophenyl)ethenyl]-HCID 5462222PotassiumHCID 130890816-Iodo-1-hexanol

생성물 1

HCID 539381646-{4-[2-(4-Nitrophenyl)ethenyl]phenoxy}hexan-1-OL

실험 절차

Employing the procedure of Example I(A), 14 g (0.05M) of the potassium salt of 4-hydroxy-4'-nitrostilbene and 14 g (0.06M) of 6-iodo-1-hexanol are reacted. The resultant product is recrystallized from toluene, m.p. 154°-157° C.

후처리

  1. customare reacted
  2. customThe resultant product is recrystallized from toluene, m.p. 154°-157° C.

출처 및 근거

ORD 기록
ord-570933961f3d452fb9b4f91af9a381f1
출처 데이터셋
uspto-grants-1989_07
특허 번호
US04851502

연결된 노트

불러오는 중…