Chloride → 2,3,4,5-Tetrafluoro-6-methylbenzoyl chloride

HRID 232654

반응식

[CH3:1][C:2]1[C:7]([C:8](O)=[O:9])=[C:6]([F:11])[C:5]([F:12])=[C:4]([F:13])[C:3]=1[F:14].[Cl-:15]>>[CH3:1][C:2]1[C:7]([C:8]([Cl:15])=[O:9])=[C:6]([F:11])[C:5]([F:12])=[C:4]([F:13])[C:3]=1[F:14]

참가 물질

반응물 2

HCID 312Chloride

HCID 129439972,3,4,5-Tetrafluoro-6-methylbenzoic acid

생성물 1

HCID 146512562,3,4,5-Tetrafluoro-6-methylbenzoyl chloride

실험 절차

To 6-methyl-2,3,4,5-tetrafluorobenzoic acid (5.60 g) is added thiony chloride (9.8 ml) and the mixture is refluxed for 1 hour. After concentrating, 6-methyl-2,3,4,5-tetrafluorobenzoyl chloride (5.20 g) is obtained as a colorless oil, b.p. 82° C./23 mmHg.

후처리

temperaturethe mixture is refluxed for 1 hour
concentrationAfter concentrating

출처 및 근거

ORD 기록: ord-e82a0650db9347bb99fe2fc522b08403
출처 데이터셋: uspto-grants-1997_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05591744

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