Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(+-)-2-Butanol → (1-Methylpropoxycarbonyl)sulfenyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (+-)-2-Butanol | HCID 6568 | — |
| 반응물 | (Chlorothio)formyl chloride | HCID 75990 | — |
| 생성물 | (1-Methylpropoxycarbonyl)sulfenyl chloride | HCID 13633290 | 39.1% |
반응 단계
Chlorocarbonylsulfenyl chloride (13.1 g, 0.1 mol) was mixed with 2-butanol (6.7 g, 0.09 mol)and warmed to about 35° to 40° C. for one hour. Distillation resulted in the tithe compound (5.93 g) Bp. 70° C./0.8 mm Hg. NMR spectrum was consistent with the structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05591764 |
| 출처 데이터셋 | uspto-grants-1997_01 |
| ORD ID | ord-61cd90b086e14eeaa59c139b8c8dc5ed |
| 출처 메모 | uspto-grants-1997_01 |