Pyrrole → N-(5-bromothiophenesulfonyl)pyrrole

HRID 234370

반응식

HRID 234370 반응식
[Br:1][C:2]1[S:6][C:5]([S:7](Cl)(=[O:9])=[O:8])=[CH:4][CH:3]=1.[NH:11]1[CH:15]=[CH:14][CH:13]=[CH:12]1>>[Br:1][C:2]1[S:6][C:5]([S:7]([N:11]2[CH:15]=[CH:14][CH:13]=[CH:12]2)(=[O:9])=[O:8])=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 8027PyrroleHCID 27339245-Bromothiophene-2-sulfonyl chloride

생성물 1

HCID 23445587N-(5-bromothiophenesulfonyl)pyrrole수율 88%

실험 절차

N-(5-bromothiophene-2-sulfonyl)pyrrole was prepared in the same manner as described in Example 33A from 5-bromothiophene-2-sulfonyl chloride and pyrrole in 88% yield. This was purified by recrystallization using hexane/ethyl acetate as a solvent.

후처리

  1. customThis was purified by recrystallization

출처 및 근거

ORD 기록
ord-ddfd046957534b878c247003914f5b75
출처 데이터셋
uspto-grants-1997_01
특허 번호
US05594021

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