Phthalic Anhydride → STK266267

HRID 2351560노트

반응식

HRID 2351560 반응식
[N+:1]([C:4]1[CH:5]=[CH:6][C:7]([NH2:11])=[C:8]([OH:10])[CH:9]=1)([O-:3])=[O:2].[C:12]1(=O)[O:17][C:15](=[O:16])[C:14]2=[CH:18][CH:19]=[CH:20][CH:21]=[C:13]12>C(O)(=O)C>[N+:1]([C:4]1[CH:5]=[CH:6][C:7]([N:11]2[C:15](=[O:16])[C:14]3=[CH:18][CH:19]=[CH:20][CH:21]=[C:13]3[C:12]2=[O:17])=[C:8]([OH:10])[CH:9]=1)([O-:3])=[O:2]

참가 물질

4

반응물 2

HCID 6811Phthalic AnhydrideHCID 49847212-Amino-5-Nitrophenol

생성물 1

HCID 4679558STK266267

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

231 g (1.5 mol) of 5-nitro-2-aminophenol and 444 g (3 mol) of phthalic acid anhydride were stirred together in 2.25 liters of acetic acid at boiling point for 2.5 hours. The product was suction filtered at room temperature, washed with water and dried. Yield: 420 g=98.5%.

후처리

  1. customfor 2.5 hours
  2. filtrationfiltered at room temperature
  3. washwashed with water
  4. customdried

출처 및 근거

ORD 기록
ord-a83c4f268ace4616bc7393fa0cb8c968
출처 데이터셋
uspto-grants-1989_10
특허 번호
US04873338

반응 노트

불러오는 중…