Methanol → HCID 54335577, 화합물
반응식
[CH2:1]([S:7][CH:8]=[CH:9][CH2:10]Cl)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].C(N(C(C)C)CC)(C)C.[CH3:21][OH:22]>CCCCCC>[CH3:21][O:22][CH2:10][CH:9]=[CH:8][S:7][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]참가 물질
5
실험 절차
3-Hexylthio-2-propenyl chloride is added to a solution of diisopropyl ethyl amine (3.68 g, 28.5 mmol) in 20 ml of methanol. The mixture is stirred overnight at RT. It is then diluted with hexane, washed with water and with brine and is stripped. The crude product is purified by prep. TLC to give 3-methoxy-1-hexylthio-1-propene.
후처리
- washwashed with water and with brine
- customThe crude product is purified by prep
출처 및 근거
- ORD 기록
- ord-3f5b6b6e640848808e565dc80061b09b
- 출처 데이터셋
- uspto-grants-1989_10
- 특허 번호
- US04877899
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