Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → Ethyl 6-(chloromethyl)picolinate hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 2-Pyridinecarboxylic acid, 6-(hydroxymethyl)-, ethyl ester | HCID 10921141 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Ethyl 6-(chloromethyl)picolinate hydrochloride | HCID 68457584 | — |
반응 단계
As for Reaction 1, using 45.14 g of ethyl 6-(hydroxymethyl)-2-pyridinecarboxylate and 33 g thionyl chloride in 500 ml dichloromethane. Yield 59.9 g
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07759369B2 |
| 출처 데이터셋 | uspto-grants-2010_07 |
| ORD ID | ord-183871bb9e68456ba638c22d39f17ad6 |
| 출처 메모 | uspto-grants-2010_07 |