HRID2356608

反应详情

EQUATION

反应方程式

HRID 2356608 的结构方程式

REACTANTS

反应物

2

结构：O=S(Cl)Cl

Thionyl chloride

Cl2OS

结构：CCOC(=O)c1cccc(CO)n1

Ethyl 6-(hydroxymethyl)pyridine-2-carboxylate

C9H11NO3

PRODUCTS

生成物

1

结构：CCOC(=O)c1cccc(CCl)n1.Cl

Ethyl 6-(chloromethyl)pyridine-2-carboxylate--hydrogen chloride (1/1)

C9H11Cl2NO2

AUXILIARIES

试剂、催化剂与溶剂

1

结构：ClCCl

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

As for Reaction 1, using 45.14 g of ethyl 6-(hydroxymethyl)-2-pyridinecarboxylate and 33 g thionyl chloride in 500 ml dichloromethane. Yield 59.9 g

WORKUP

后处理

customAs for Reaction 1