3-(3-Nitrophenyl)prop-2-enal → 3-nitrocinnamaldehyde Thiosemicarbazone

HRID 2362834노트

반응식

HRID 2362834 반응식
[N+:1]([C:4]1[CH:5]=[C:6]([CH:11]=[CH:12][CH:13]=1)[CH:7]=[CH:8][CH:9]=O)([O-:3])=[O:2].[NH2:14][NH:15][C:16]([NH2:18])=[S:17]>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:11]=[CH:12][CH:13]=1)[CH:7]=[CH:8][CH:9]=[N:14][NH:15][C:16]([NH2:18])=[S:17])([O-:3])=[O:2]

참가 물질

3

반응물 2

HCID 2664543-(3-Nitrophenyl)prop-2-enalHCID 2723789Thiosemicarbazide

생성물 1

HCID 866333063-nitrocinnamaldehyde Thiosemicarbazone수율 88%

실험 절차

The compound is prepared according to the method described in Example 1A from 3-nitrocinnamaldehyde (2.2 mmol) (Org. Lett. 5(5), 777-780, 2003) and from thiosemicarbazide (2.2 mmol). Yield 88%.

후처리

  1. customThe compound is prepared

출처 및 근거

ORD 기록
ord-40a79d62a0e649a2bb29c23a3e779dba
출처 데이터셋
uspto-grants-2014_04
특허 번호
US08691854B2

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