Hydrochloric Acid → Diisopropylamino-acetic acid hydrochloride

HRID 2364929노트

반응식

HRID 2364929 반응식
C([O:5][C:6](=[O:15])[CH2:7][N:8]([CH:12]([CH3:14])[CH3:13])[CH:9]([CH3:11])[CH3:10])(C)(C)C.[ClH:16]>O>[ClH:16].[CH:9]([N:8]([CH2:7][C:6]([OH:15])=[O:5])[CH:12]([CH3:13])[CH3:14])([CH3:10])[CH3:11]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 11333389HCID 11333389, 화합물

생성물 1

HCID 46735981Diisopropylamino-acetic acid hydrochloride

시약·촉매·용매 1

HCID 962Water용매

실험 절차

5.4 g (25 mMol) diisopropylamino-acetic acid tert-butylester 2 was stirred with 6.25 ml (75 mMol) 12 M HCl in 25 ml water for 2.5 h at 60° C. After distillation in vacuo of water and excess of HCl, the residue was dried with toluene azeotropically.

후처리

  1. distillationAfter distillation in vacuo of water
  2. dry with materialexcess of HCl, the residue was dried with toluene azeotropically

출처 및 근거

ORD 기록
ord-ebb2f625df644252aacb55878745cfe1
출처 데이터셋
uspto-grants-2014_04
특허 번호
US08697604B2

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