Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Citronellyl Acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Hexane | HCID 8058 | — |
| 생성물 | Citronellyl Acetate | HCID 9017 | — |
반응 단계
To 15.6 g (0.1 mol) d1-citronellol in 20 ml of dry pyridine under nitrogen is added 11.3 ml (0.12 mol) of acetic anhydride. The reaction is stirred about 48 hours and then ice is added. After one hour, the reaction is poured into hexane and water. The organic phase is washed with 5% HCl, 2M sodium carbonate, and saturated NaCl solutions, dried over calcium sulfate and solvent removed to yield dl-citronellyl acetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04158096 |
| 출처 데이터셋 | uspto-grants-1979_06 |
| ORD ID | ord-3ddca04c8f4a4b5885d7d10c1ae64d52 |
| 출처 메모 | uspto-grants-1979_06 |