反应详情

To 15.6 g (0.1 mol) d1-citronellol in 20 ml of dry pyridine under nitrogen is added 11.3 ml (0.12 mol) of acetic anhydride. The reaction is stirred about 48 hours and then ice is added. After one hour, the reaction is poured into hexane and water. The organic phase is washed with 5% HCl, 2M sodium carbonate, and saturated NaCl solutions, dried over calcium sulfate and solvent removed to yield dl-citronellyl acetate.

1. additionice is added
2. waitAfter one hour
3. washThe organic phase is washed with 5% HCl, 2M sodium carbonate, and saturated NaCl solutions
4. dry with materialdried over calcium sulfate and solvent
5. customremoved