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Hydrochloric Acid → Procromil

HRID 236948
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인쇄 미리보기

반응식

HRID 236948 반응식
[O:1]=[C:2]1[CH:7]=[C:6]([C:8]([O-:10])=[O:9])[O:5][C:4]2[C:11]([CH2:19][CH2:20][CH3:21])=[C:12]3[C:17](=[CH:18][C:3]1=2)[CH2:16][CH2:15][CH2:14][CH2:13]3.[Na+].Cl>O>[O:1]=[C:2]1[CH:7]=[C:6]([C:8]([OH:10])=[O:9])[O:5][C:4]2[C:11]([CH2:19][CH2:20][CH3:21])=[C:12]3[C:17](=[CH:18][C:3]1=2)[CH2:16][CH2:15][CH2:14][CH2:13]3
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 23717002HCID 23717002, 화합물

생성물 1

HCID 3085184Procromil수율 86.1%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A solution of the product of step (e) (0.3 g), in water (25 ml) was acidified with 2 N hydrochloric acid. The precipitated organic acid was filtered off washed with water and dried to give the title compound as a white solid, (0.24 g), mp 245°-8°.

후처리

  1. filtrationThe precipitated organic acid was filtered off
  2. washwashed with water
  3. customdried

출처 및 근거

ORD 기록
ord-2ab03829606f4b1082ec121ea5be184d
출처 데이터셋
uspto-grants-1979_06
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04159273

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