Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(3-Chlorophenyl)piperazine → 1-(3-Chlorophenyl)-4-(4-nitrophenyl)sulfonylpiperazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(3-Chlorophenyl)piperazine | HCID 1355 | — |
| 반응물 | 4-Nitrobenzenesulfonyl chloride | HCID 7404 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 1-(3-Chlorophenyl)-4-(4-nitrophenyl)sulfonylpiperazine | HCID 1019725 | — |
반응 단계
In the manner given in Example 1A, p-nitrobenzenesulfonyl chloride, 1-(m-chlorophenyl)piperazine, and triethylamine are stirred at reflux to give 1-[(p-nitrophenyl)sulfonyl]-4-(m-chlorophenyl)piperazine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04159331 |
| 출처 데이터셋 | uspto-grants-1979_06 |
| ORD ID | ord-dd6266a2b2ba43b992466510e0d45622 |
| 출처 메모 | uspto-grants-1979_06 |