HRID237024

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID1355

1-(3-Chlorophenyl)piperazine

C10H13ClN2

HCID7404

Benzenesulfonyl chloride, 4-nitro-

C6H4ClNO4S

PRODUCTS

生成物

结构：O=[N+]([O-])c1ccc(S(=O)(=O)N2CCN(c3cccc(Cl)c3)CC2)cc1

HCID1019725

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

In the manner given in Example 1A, p-nitrobenzenesulfonyl chloride, 1-(m-chlorophenyl)piperazine, and triethylamine are stirred at reflux to give 1-[(p-nitrophenyl)sulfonyl]-4-(m-chlorophenyl)piperazine.

WORKUP

后处理

temperatureat reflux