Ethanol → HCID 19907417, 화합물
반응식
[CH2:1]([N:3]([CH2:21][CH3:22])[CH2:4][CH2:5][CH2:6][C:7]1[CH:12]=[CH:11][C:10]([CH2:13][CH2:14][CH2:15][N:16]([CH2:19][CH3:20])[CH2:17][CH3:18])=[CH:9][CH:8]=1)[CH3:2].[CH2:23]([I:25])[CH3:24].[CH2:26](O)[CH3:27]>>[I-:25].[I-:25].[CH2:19]([N+:16]([CH2:23][CH3:24])([CH2:17][CH3:18])[CH2:15][CH2:14][CH2:13][C:10]1[CH:9]=[CH:8][C:7]([CH2:6][CH2:5][CH2:4][N+:3]([CH2:26][CH3:27])([CH2:1][CH3:2])[CH2:21][CH3:22])=[CH:12][CH:11]=1)[CH3:20]참가 물질
4
실험 절차
304 mg of 1,4-bis(3-diethylaminopropyl)benzene was dissolved in 2.5 ml of absolute ethanol, and after dropwise addition of 1.56 g of ethyl iodide, the mixture was refluxed for 1.5 hours in dark. After cooling, ethanol was partially removed under reduced pressure, the resulting crystal was filtered, quickly washed with ethanol and dried in vacuo to obtain 461 mg of the title compound as a colorless crystal.
후처리
- temperaturethe mixture was refluxed for 1.5 hours in dark
- temperatureAfter cooling
- custom