Aniline → 3-Phenylammonio-1-propanesulfonate
반응식
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:8]1[S:12](=[O:14])(=[O:13])[O:11][CH2:10][CH2:9]1>C(#N)C>[C:2]1([NH2+:1][CH2:10][CH2:9][CH2:8][S:12]([O-:14])(=[O:13])=[O:11])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1참가 물질
4
실험 절차
A mixture of aniline (7 mmol) and propane sultone (10 mmol) was heated in 10 mL of acetonitrile at 12.0-130° C. for 9 h in a pressure tube under argon atmosphere. The product was allowed to cool to room temperature and the solid of 3-phenylammonio-1-propanesulfonate was filtered and air-dried. Yield: 95%.
후처리
- filtrationthe solid of 3-phenylammonio-1-propanesulfonate was filtered
- customair-dried
출처 및 근거
- ORD 기록
- ord-f03ab8001ee74a3fa69d20bb82c32bc4
- 출처 데이터셋
- uspto-grants-2014_02
- 특허 번호
- US08642014B2
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