Ethylenediamine → N~1~-(Pyridin-2-yl)ethane-1,2-diamine

HRID 238498

반응식

HRID 238498 반응식
[CH2:1]([NH2:4])[CH2:2][NH2:3].F[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][N:7]=1>>[N:7]1[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=1[NH:3][CH2:2][CH2:1][NH2:4]

참가 물질

3

반응물 2

HCID 3301EthylenediamineHCID 97462-Fluoropyridine

생성물 1

HCID 410428N~1~-(Pyridin-2-yl)ethane-1,2-diamine

실험 절차

Ethylenediamine (6 g, 0.1 mol) and 2-fluoropyridine (10 g, 0.1 mol) were heated neat at 120° C. overnight. The reaction was cooled and the residue was used in next step without further purification.

후처리

  1. temperatureThe reaction was cooled
  2. customthe residue was used in next step without further purification

출처 및 근거

ORD 기록
ord-d13c71bd5af9458eb262afc0d4dc0739
출처 데이터셋
uspto-grants-2014_02
특허 번호
US08642624B2

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