Acetic Anhydride → HCID 23359034, 화합물

HRID 2396955노트

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HRID 2396955 반응식
[F:1][C:2]1[C:8]([CH3:9])=[C:7]([F:10])[C:6]([F:11])=[CH:5][C:3]=1[NH2:4].[C:12](OC(=O)C)(=[O:14])[CH3:13]>>[F:1][C:2]1[C:8]([CH3:9])=[C:7]([F:10])[C:6]([F:11])=[CH:5][C:3]=1[NH:4][C:12](=[O:14])[CH3:13]

참가 물질

3

반응물 2

HCID 7918Acetic AnhydrideHCID 146512532,4,5-Trifluoro-3-methylaniline

생성물 1

HCID 23359034HCID 23359034, 화합물

실험 절차

To 2,4,5-trifluoro-3-methylaniline (1 g) is added acetic anhydride (3 ml) at room temperature with stirring and the mixture is stirred for 15 minutes. The reaction mixture is poured into ice-water, extracted with dichloromethane, and the extract is washed with water and dried. The solvent is distilled off to give 2,4,5-trifluoro-3-methyl-N-acetylaniline (1.14 g), as white crystals.

후처리

  1. stirringthe mixture is stirred for 15 minutes
  2. extractionextracted with dichloromethane
  3. washthe extract is washed with water
  4. customdried
  5. distillationThe solvent is distilled off

출처 및 근거

ORD 기록
ord-c2cebb32e5a141fab7892d3f84c4c075
출처 데이터셋
uspto-grants-1996_02
특허 번호
US05495020

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