Cyclohexylamine → HCID 23005249, 화합물

HRID 2397387노트

반응식

HRID 2397387 반응식
[Cl:1][C:2]1[CH:3]=[C:4]([C:8]2[CH:13]=[CH:12][C:11]([CH:14](O)[CH2:15][CH2:16][C:17]([OH:19])=[O:18])=[CH:10][CH:9]=2)[CH:5]=[CH:6][CH:7]=1.C1(N)CCCCC1>>[Cl:1][C:2]1[CH:3]=[C:4]([C:8]2[CH:13]=[CH:12][C:11]([CH2:14][CH2:15][CH2:16][C:17]([OH:19])=[O:18])=[CH:10][CH:9]=2)[CH:5]=[CH:6][CH:7]=1

참가 물질

3

반응물 2

HCID 7965CyclohexylamineHCID 21437961HCID 21437961, 화합물

생성물 1

HCID 23005249HCID 23005249, 화합물수율 41%

실험 절차

Prepared analogous to Example 9 from 4-(3'-chloro-4-biphenylyl)-4-hydroxy-butyric acid. Melting point of the cyclohexylamine salt: 147°-148° C. Yield: 41% of theory.

후처리

  1. custom147°-148° C

출처 및 근거

ORD 기록
ord-8cc1129e4f2e4ae781074de2559ecd34
출처 데이터셋
uspto-grants-1977_05
특허 번호
US04021479

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