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Sodium Hydroxide → HCID 131710746, 화합물

HRID 2398012
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HRID 2398012 반응식
[OH-:1].[Na+:2].[CH2:3]1[N:8]2[CH2:9][N+:10]3([CH2:13]/[CH:14]=[CH:15]\[Cl:16])[CH2:12][N:6]([CH2:7]2)[CH2:5][N:4]1[CH2:11]3.[Cl-:17]>O>[CH2:5]1[N:4]2[CH2:11][N+:10]3([CH2:13]/[CH:14]=[CH:15]\[Cl:16])[CH2:9][N:8]([CH2:3]2)[CH2:7][N:6]1[CH2:12]3.[Cl-:17].[OH-:1].[Na+:2]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 14798Sodium HydroxideHCID 6435993cis-1-(3-Chloroallyl)-3,5,7-triaza-1-azoniaadamantane chloride

생성물 1

HCID 131710746HCID 131710746, 화합물수율 78%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Excess sodium hydroxide, preferably, 4 molar proportions, is dissolved in water and cooled to room temperature. A quantity of about one mole of Dowicil 200 antimicrobial is added slowly to the caustic solution and the reaction mixture is stirred approximately 15 minutes at ambient temperature. The ⟦Carbinolamine⟧ basic oil which forms is extracted with benzene, the extract is dried over sodium sulfate and the benzene is evaporated to give the ⟦Carbinolamine⟧ basic oil in an approximately 78% yield as a viscous oil.

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후처리

  1. extractionThe ⟦Carbinolamine⟧ basic oil which forms is extracted with benzene
  2. dry with materialthe extract is dried over sodium sulfate
  3. customthe benzene is evaporated
  4. customto give the ⟦Carbinolamine⟧ basic oil in an approximately 78% yield as a viscous oil

출처 및 근거

ORD 기록
ord-b054eaaa1f744db2bd0e7afea90833ee
출처 데이터셋
uspto-grants-1977_05
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
USRE029225

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