Glycine → L-Methionyl-L-valine

HRID 2398322노트

반응식

HRID 2398322 반응식
[NH2:1][CH:2]([C:7]([OH:9])=O)[CH2:3][CH2:4][S:5][CH3:6].NCC(O)=O.N[C@H](C(O)=O)CCSC.[NH2:24][C@H:25]([C:29]([OH:31])=[O:30])[CH:26]([CH3:28])[CH3:27]>O>[NH2:1][C@H:2]([C:7]([NH:24][C@H:25]([C:29]([OH:31])=[O:30])[CH:26]([CH3:28])[CH3:27])=[O:9])[CH2:3][CH2:4][S:5][CH3:6]

참가 물질

6

반응물 4

HCID 750GlycineHCID 876(+-)-MethionineHCID 6137L-Methionine2회HCID 6287L-Valine2회

생성물 1

HCID 7010520L-Methionyl-L-valine

시약·촉매·용매 1

HCID 962Water용매

실험 절차

The title compound was prepared according to the procedure of Example 1A and B above by replacing DL-methionine and glycine respectively with L-methionine and L-valine (Aldrich Chemical Co., Beil 4,427). The title compound had a melting point of 227° to 229° C (d). The title compound was found to be water soluble. The product thus obtained was subjected to amino acid analysis and found to contain 49.44 mole percent valine and 50.56 mole percent methionine.

후처리

  1. customThe title compound was prepared
  2. customThe product thus obtained

출처 및 근거

ORD 기록
ord-05dc351208bb485da6bc199c65ae48f3
출처 데이터셋
uspto-grants-1977_05
특허 번호
US04024286

반응 노트

불러오는 중…