Formamide → HCID 178518065, 화합물

반응식

C([O:3][C:4]([C:6]1[C:7]2[CH:15]=[CH:14][CH:13]=[CH:12][C:8]=2[S:9][C:10]=1[NH2:11])=O)C.[CH:16]([NH2:18])=O>>[N:11]1[C:10]2[S:9][C:8]3[CH:12]=[CH:13][CH:14]=[CH:15][C:7]=3[C:6]=2[C:4]([OH:3])=[N:18][CH:16]=1

참가 물질

반응물 2

HCID 713Formamide

HCID 699464Ethyl 2-amino-1-benzothiophene-3-carboxylate

생성물 1

HCID 178518065HCID 178518065, 화합물

실험 절차

The solution of 10 millimol IX in 15 milliliter milliliter formamide was stirred at 100° C. for 3 hours then cooled down to room temperature. The reaction mixture was poured onto crushed ice with continuous stirring then collected by filtration. The product was washed with water and n-hexane, then dried.

후처리

additionThe reaction mixture was poured
customonto crushed ice
filtrationthen collected by filtration
washThe product was washed with water and n-hexane
customdried

출처 및 근거

ORD 기록: ord-fcd1f227558b4307b108c50fdc9d3f9d
출처 데이터셋: uspto-grants-2014_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08802849B2

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