Methyl iodide → 3,5-Dimethyl-2,4-Imidazolidinedione

반응식

[CH3:1][CH:2]1[NH:6][C:5](=[O:7])[NH:4][C:3]1=[O:8].[CH3:9]I>>[CH3:9][N:4]1[C:3](=[O:8])[CH:2]([CH3:1])[NH:6][C:5]1=[O:7]

참가 물질

반응물 2

HCID 6328Methyl iodide

HCID 692165-Methylhydantoin

생성물 1

HCID 101540613,5-Dimethyl-2,4-Imidazolidinedione

실험 절차

Using 5-methylimidazolidine-2,4-dione (1.00 g) and methyl iodide (0.57 mL) and by the reaction and treatment in the same manner as in Preparation Example 214, the title compound (1.66 g, containing DMF) was obtained.

후처리

customby the reaction and treatment in the same manner
customas in Preparation Example 214

출처 및 근거

ORD 기록: ord-6a391b4510b048bf8b2cb1df12641ef4
출처 데이터셋: uspto-grants-2014_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08816079B2

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