Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Nitropropane → 5-methoxy-3-(2,2-dimethyl-2-nitroethyl)-1H-indole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Nitropropane | HCID 398 | — |
| 반응물 | 5-Methoxy-N,N-dimethyl-1H-indole-3-methanamine | HCID 27965 | — |
| 생성물 | 5-methoxy-3-(2,2-dimethyl-2-nitroethyl)-1H-indole | HCID 12619662 | — |
반응 단계
This material was prepared by the reaction of 5-methoxygramine (Procedure 11B) and 2-nitropropane substantially as described in Procedure 10C. The product was initially recovered as a dark oil which crystallized from i-Pr2O solution after treatment thereof with activated carbon, yield 31.3 g. (from 33 g. of 5-methoxygramine), m.p. 83°-85°. The identity of the product was confirmed by inspection of its NMR spectrum.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04495352 |
| 출처 데이터셋 | uspto-grants-1985_01 |
| ORD ID | ord-3961d4c57a6742818b9fe5f8135a5555 |
| 출처 메모 | uspto-grants-1985_01 |