反应详情

This material was prepared by the reaction of 5-methoxygramine (Procedure 11B) and 2-nitropropane substantially as described in Procedure 10C. The product was initially recovered as a dark oil which crystallized from i-Pr2O solution after treatment thereof with activated carbon, yield 31.3 g. (from 33 g. of 5-methoxygramine), m.p. 83°-85°. The identity of the product was confirmed by inspection of its NMR spectrum.

1. customThe product was initially recovered as a dark oil which
2. customcrystallized from i-Pr2O solution after treatment