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Ethanol → Ethyl bis(pentafluoroethyl)phosphinite

HRID 241310
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인쇄 미리보기

반응식

HRID 241310 반응식
[F:1][C:2]([P:8](Cl)[C:9]([F:15])([F:14])[C:10]([F:13])([F:12])[F:11])([F:7])[C:3]([F:6])([F:5])[F:4].[CH2:17]([OH:19])[CH3:18]>CN(C)C1C=CN=CC=1.C(OCC)C>[F:1][C:2]([P:8]([C:9]([F:15])([F:14])[C:10]([F:13])([F:12])[F:11])[O:19][CH2:17][CH3:18])([F:7])[C:3]([F:6])([F:5])[F:4]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 2

HCID 702EthanolHCID 2757428Bis(pentafluoroethyl)phosphinous chloride2회

생성물 1

HCID 86653812Ethyl bis(pentafluoroethyl)phosphinite

시약·촉매·용매 2

HCID 142844-(Dimethylamino)pyridine촉매HCID 3283Diethyl Ether용매

실험 절차

Bis(pentafluoroethyl)phosphinous acid chloride, (C2F5)2PCl, obtainable in accordance with Example 2, is added to a mixture of ethanol and 4-dimethylaminopyridine in diethyl ether at room temperature. The precipitated product 4-dimethylaminopyridinium chloride is separated off, and the solution comprises ethyl bis(pentafluoroethyl)phosphinite, (C2F5)2POC2H5.

후처리

  1. customThe precipitated product 4-dimethylaminopyridinium chloride is separated off

출처 및 근거

ORD 기록
ord-eda27c680cc84ed38fcae7051d4ad4c6
출처 데이터셋
uspto-grants-2014_02
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US08648202B2

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