2-Amino-2-methyl-1,3-propanediol → 2-(((10-(2-Methoxyethoxy)-9-anthracenyl)methyl)amino)-2-methyl-1,3-propanediol hydrochloride

HRID 2413649

반응식

HRID 2413649 반응식
CS(O)(=O)=O.[Cl:6]C1C2C(=CC=CC=2)C(CNC(O)C(C)CO)=C2C=1C=CC=C2.[CH3:29][O:30][CH2:31][CH2:32][O:33][C:34]1[C:47]2[C:42](=[CH:43][CH:44]=[CH:45][CH:46]=2)[C:41]([CH:48]=O)=[C:40]2[C:35]=1[CH:36]=[CH:37][CH:38]=[CH:39]2.[NH2:50][C:51]([CH3:56])([CH2:54][OH:55])[CH2:52][OH:53]>>[ClH:6].[CH3:29][O:30][CH2:31][CH2:32][O:33][C:34]1[C:35]2[C:40](=[CH:39][CH:38]=[CH:37][CH:36]=2)[C:41]([CH2:48][NH:50][C:51]([CH3:56])([CH2:54][OH:55])[CH2:52][OH:53])=[C:42]2[C:47]=1[CH:46]=[CH:45][CH:44]=[CH:43]2

참가 물질

4

반응물 3

HCID 15312-Amino-2-methyl-1,3-propanediolHCID 1337540710-(2-Methoxyethoxy)9-anthracenecarbaldehydeHCID 86741972HCID 86741972, 화합물

생성물 1

HCID 212762482-(((10-(2-Methoxyethoxy)-9-anthracenyl)methyl)amino)-2-methyl-1,3-propanediol hydrochloride

실험 절차

Using the reductive amination procedure outlined in 2B, (10-methoxyethoxy)anthracene-9-carbaldehyde (27A) and 2-amino-2-methyl-1,3-propanediol gave 2-(((10-(2-methoxyethoxy)-9-anthracenyl)methyl)amino)-2-methyl-1,3-propanediol hydrochloride.1/4H2O mp 182°-183° (dec), (EtOH/Et2O), (C, H, Cl, N).

출처 및 근거

ORD 기록
ord-06ed79b9cc3f4fd5aa3dd5ac2b88a999
출처 데이터셋
uspto-grants-1988_01
특허 번호
US04719049

연결된 노트

불러오는 중…