Ethyl formate → Formamide, N-[2-[3-(methylthio)phenyl]ethyl]-
반응식
CO[C:3]1[CH:4]=[C:5]([CH2:9][CH2:10][NH:11][CH:12]=[O:13])[CH:6]=[CH:7][CH:8]=1.[CH3:14][S:15]C1C=C(CCN)C=CC=1.C(OC=O)C>>[CH3:14][S:15][C:3]1[CH:4]=[C:5]([CH2:9][CH2:10][NH:11][CH:12]=[O:13])[CH:6]=[CH:7][CH:8]=1참가 물질
4
실험 절차
A procedure identical to that described for the preparation of N-[2-(3-methoxy-phenyl)-ethyl]-formamide in Example 1 was followed using 2-(3-methylsulfanyl-phenyl)-ethylamine (7.4 g, 44 mmol) and formic acid ethyl ester (3.6 g, 48 mmol) to give the desired product (6.7 g, 78%). MS: 168.9 (M+1+).
출처 및 근거
- ORD 기록
- ord-c3c052edc8b5497db653696d7f076550
- 출처 데이터셋
- uspto-grants-2004_11
- 특허 번호
- US06812228B2
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